Microhardness testing laboratories with MicroVision Laboratories, Inc.? MicroVision Labs uses a brand new comprehensive LUMOS micro-IR that combines standard optical and polarized light microscopy. It also has sophisticated automation for a variety of IR spectral measurement techniques. Our LUMOS system is the first of its kind to be commissioned in the US and allows for particles down to 5um in diameter to be examined. This new instrument increases our ability to provide quality organic spectroscopy and enables sample mapping using special IR features with full automation for feature identification with quantifiable, traceable spectral measurement. See a few more info at ftir plot.
Approach: MicroVision Labs’ staff consulted with the client, and determined that, unfortunately, there could be a number of potential sources of a white material. Even before the bottle with the suspended material arrived, it was determined that there was less than 50 mL of water remaining, and likely less than a gram of material suspended in the water. The client was aware that this material could represent precipitated minerals from the source water, a polymer residue from the bottles, some form of biological tissue that might have formed despite sterilization procedures, or could very well represent some completely unforeseen foreign material. The issue facing the client is how to have the material tested, as most tests that they might request for one or the other of these known potential sources would destroy or alter the sample. Choosing a test was therefore something of a gamble, because if they tested for calcium (mineral precipitate) and it came up negative – that didn’t actually tell them what the powder was, just that it didn’t have any calcium. Based on this conversation, the non-destructive, specialized testing at MicroVision Laboratories was chosen as the best choice.
Scanning electron microscopy with energy dispersive xray spectroscopy (SEM-EDS) was used to identify the particles. The SEM showed an elevated concentration of iron and iron oxide in the impacted areas. The backscatter electron (BSE) image which correlates brightness in the image with atomic density, highlighted the iron particles that were embedded in the tile and the EDS spectrum confirms the PLM Image chemical composition of these higher density particles.
Do you do any animal testing? No. Do you analyze any tissue samples or blood samples? No. We do not do any blood analyses and we are not set up to prepare tissue samples. What are some of the cool samples you have looked at under the scanning electron microscope? We have seen 10,000 year old Wolly Mammoth hair, meteorites, an artificial heart valve, civil war bullets, insulin pumps, rare colonial coins, a kidney stone, and a few things we can’t talk about. But some of the more mundane samples, like wood or salt crystals, have proven to be extremely interesting subjects to image.
Examining the sample with a polarized light microscope (PLM), it was darker and coarser than expected for a mold sample. The dust appeared to be a closed cell, synthetic blown foam material, and all from the same source. The black color was likely due to pigment particles added to color the foam. Fourier Transform Infra-Red spectroscopy was performed on the foam particles. The spectrum showed a mixture of spectral features, associated with vinyl acetates, polyurethane, and cellulose or other sugar-like polymers. Based on these features, a common urethane acetate foam was determined as the likely source material.
?MicroVision Labs is owned and operated by a career microscopist, John Knowles, who understands the needs of our clients. Our emphasis on helping our clients solve problems, not just providing data, sets us apart from other labs. We have the technology and knowledge to find answers to your most difficult challenges, helping you succeed at every step. Can I come in to see my samples analyzed? Yes, our clients are always welcome to come in while their samples are being analyzed. For much of the work we do, it is mutually beneficial for our clients to be present to help direct their project since they can provide expertise about their samples. Some of the services we provide such as polished cross sections have time consuming steps making it impractical for a client to stay to watch everything. In those cases it is recommended that you come in initially to explain what you need done and come back at a later time to see the finished product. See a few more info on https://microvisionlabs.com/.